C₁₁H₉FN₂O₄S

Base Information

Chemical Name:C₁₁H₉FN₂O₄S
CAS No.:936129-51-0
Molecular Formula:C₁₁H₉FN₂O₄S
Molecular Weight:284.268
Hs Code.:

C<sub>11</sub>H<sub>9</sub>FN<sub>2</sub>O<sub>4</sub>S

Synonyms:C₁₁H₉FN₂O₄S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₁H₉FN₂O₄S

Chemical Property:

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Technology Process of C₁₁H₉FN₂O₄S

There total 4 articles about C₁₁H₉FN₂O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1422176-18-8
C₁₁H₉FN₂O₃S

: 936129-51-0
C₁₁H₉FN₂O₄S

Guidance literature:: With potassium peroxymonosulfate; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield:

: 403-42-9
1-(4-fluorophenyl)ethanone

: 936129-51-0
C₁₁H₉FN₂O₄S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium acetate / ethanol / 1 h / 1 °C / Reflux

1.2: Reflux

2.1: trichlorophosphate / 1 h / 0 - 20 °C

2.2: 2 h / 80 °C / Cooling with ice

2.3: Cooling with ice

3.1: pyridine / 22 h / 60 °C

4.1: potassium peroxymonosulfate / N,N-dimethyl-formamide / 20 °C

With pyridine; potassium peroxymonosulfate; potassium acetate; trichlorophosphate; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 326-33-0
4-fluoroacetophenone semicarbazone

: 936129-51-0
C₁₁H₉FN₂O₄S

Guidance literature:: Multi-step reaction with 3 steps

1.1: trichlorophosphate / 1 h / 0 - 20 °C

1.2: 2 h / 80 °C / Cooling with ice

1.3: Cooling with ice

2.1: pyridine / 22 h / 60 °C

3.1: potassium peroxymonosulfate / N,N-dimethyl-formamide / 20 °C

With pyridine; potassium peroxymonosulfate; trichlorophosphate; In N,N-dimethyl-formamide;