C₁₃H₁₈O

Base Information

Chemical Name:C₁₃H₁₈O
CAS No.:860455-44-3
Molecular Formula:C₁₃H₁₈O
Molecular Weight:190.285
Hs Code.:

Synonyms:C₁₃H₁₈O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₈O

Chemical Property:

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Technology Process of C₁₃H₁₈O

There total 2 articles about C₁₃H₁₈O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2305-21-7
2-hexen-1-ol

: 100-39-0
benzyl bromide

: 860455-44-3
C₁₃H₁₈O

Guidance literature:: 2-hexen-1-ol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 ℃; for 0.75h; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; for 24h; Inert atmosphere;
DOI:10.1039/d1ob01649k

Reference yield:

: 811-49-4
ethyllithium

: (((4-bromobut-2-en-1-yl)oxy)methyl)benzene

: 860455-44-3
C₁₃H₁₈O

: C₁₃H₁₈O

Guidance literature:: (((4-bromobut-2-en-1-yl)oxy)methyl)benzene; With copper(I) bromide dimethylsulfide complex; C₄₃H₄₀FeNP₂⁽²⁺⁾; In dichloromethane; toluene; at -80 ℃; Inert atmosphere;

ethyllithium; In hexane; dichloromethane; at -80 ℃; optical yield given as %ee; enantioselective reaction;
DOI:10.1038/nchem.1009

Reference yield: 91.0%

: 860455-44-3
C₁₃H₁₈O

: (2S,3S)-1-(benzyloxy)hexane-2,3-diol

Guidance literature:: With osmium(VIII) oxide; methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; 4-[(R)-[(2R,4R,5S)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]-(6-methoxy-4-quinolinyl)methoxy]-1-[(R)-[(2R,4S,5R)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]-(6-methoxy-4-quinolinyl)methoxy]phthalazine; potassium hexacyanoferrate(III); In water; tert-butyl alcohol; at 0 ℃; for 52h; Inert atmosphere;
DOI:10.1039/d1ob01649k