C₄₂H₂₃Br

Base Information

Chemical Name:C₄₂H₂₃Br
CAS No.:1233876-96-4
Molecular Formula:C₄₂H₂₃Br
Molecular Weight:607.549
Hs Code.:

Synonyms:C₄₂H₂₃Br

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Chemical Property of C₄₂H₂₃Br

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Technology Process of C₄₂H₂₃Br

There total 5 articles about C₄₂H₂₃Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.3%

: 616235-15-5
benzo{[f]-4,7-diphenyl}-indeno[1,2,3-cd]perylene

: 1233876-96-4
C₄₂H₂₃Br

Guidance literature:: With N-Bromosuccinimide; In N,N-dimethyl-formamide; at 20 ℃; for 6h;

Reference yield: 59.0%

: 1400556-26-4
C₄₂H₂₅Br

: 1233876-96-4
C₄₂H₂₃Br

Guidance literature:: With aluminum (III) chloride; In chlorobenzene; at 30 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 7267-03-0
5-bromoacenaphthylene

: 1233876-96-4
C₄₂H₂₃Br

Guidance literature:: Multi-step reaction with 5 steps

1.1: 5,5-dimethyl-1,3-cyclohexadiene / 24 h / Reflux

2.1: acetic acid; hydrogen bromide / 12 h / Reflux

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene; ethanol; water / 12 h / 90 °C

4.1: trifluoroacetic acid; boron trifluoride diethyl etherate; 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1 h / 20 °C / Inert atmosphere

4.2: 1 h / Inert atmosphere

5.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 6 h / 20 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron trifluoride diethyl etherate; hydrogen bromide; sodium carbonate; acetic acid; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; water; N,N-dimethyl-formamide; toluene;