2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

Base Information

Chemical Name:2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on
CAS No.:78476-97-8
Molecular Formula:C₂₂H₂₆N₂O₅
Molecular Weight:398.459
Hs Code.:

2-<Cyclohexyl-(4-nitrobenzoyl)amino>-6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

Synonyms:2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

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Chemical Property of 2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

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Technology Process of 2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

There total 8 articles about 2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 78477-05-1
2--6-hydroxy-4,4-dimethyl-2,5-cyclohexadien-1-on

: 80-48-8
methyl p-toluene sulfonate

: 78476-97-8
2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

Guidance literature:: With sodium hydride; In acetonitrile; at 50 ℃; for 5h;

Reference yield:

: 78477-02-8
2-(Benzyloxycarbonyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

: 78476-97-8
2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

Guidance literature:: Multi-step reaction with 4 steps

1: 82 percent / glac. CH₃COOH, H₂ / 10 percent Pd/C / ethanol / 1 h / further reagent: KOH

2: 91 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 1 h / Ambient temperature

3: 72 percent / 70 percent NaH / acetonitrile / 2.5 h / 40 °C

4: 68 percent / 70 percent NaH / acetonitrile / 5 h / 50 °C

With hydrogen; sodium hydride; acetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; palladium on activated charcoal; In ethanol; acetonitrile; benzene;

Reference yield:

: 78477-00-6
2-(4-Nitrobenzoyloxy)-3-cyclohexylamino-5,5-dimethyl-2-cyclohexen-1-on

: 78476-97-8
2--6-methoxy-4,4-dimethyl-2,5-cyclohexadien-1-on

Guidance literature:: Multi-step reaction with 2 steps

2: 68 percent / 70 percent NaH / acetonitrile / 5 h / 50 °C

With sodium hydride; In acetonitrile;