2-(2-Bromophenyl)ethanethioamide

Base Information

Chemical Name:2-(2-Bromophenyl)ethanethioamide
CAS No.:103317-32-4
Molecular Formula:C₈H₈BrNS
Molecular Weight:230.128
Hs Code.:2924190090
DSSTox Substance ID:DTXSID001308241
Mol file:103317-32-4.mol

Synonyms:2-(2-bromophenyl)ethanethioamide;2-(2-Bromophenyl)thioacetamide;103317-32-4;2-Bromobenzeneethanethioamide;SCHEMBL5060693;RITRBTUNNIPGOB-UHFFFAOYSA-N;2-(2-bromo-phenyl)-thioacetamide;DTXSID001308241;MFCD09816252;AKOS000159793;AS-5408;CS-0440041;EN300-1263919

Suppliers and Price of 2-(2-Bromophenyl)ethanethioamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-(2-Bromophenyl)ethanethioamide
100mg
$ 45.00

TRC
2-(2-Bromophenyl)ethanethioamide
1g
$ 115.00

SynQuest Laboratories
2-(2-Bromophenyl)thioacetamide
1 g
$ 168.00

Matrix Scientific
2-(2-Bromophenyl)thioacetamide 95+%
1g
$ 246.00

Crysdot
2-(2-Bromophenyl)thioacetamide 95+%
10g
$ 395.00

Atlantic Research Chemicals
2-(2-Bromophenyl)ethanethioamide 95%
1gm:
$ 95.43

Apolloscientific
2-(2-Bromophenyl)thioacetamide
1g
$ 142.00

AK Scientific
2-(2-Bromophenyl)ethanethioamide
5g
$ 371.00

Total 3 raw suppliers

Chemical Property of 2-(2-Bromophenyl)ethanethioamide

Chemical Property:

XLogP3:2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:228.95608
Heavy Atom Count:11
Complexity:149

Purity/Quality:

98%min ^*data from raw suppliers

2-(2-Bromophenyl)ethanethioamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)CC(=S)N)Br

Technology Process of 2-(2-Bromophenyl)ethanethioamide

There total 4 articles about 2-(2-Bromophenyl)ethanethioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 19472-74-3
2-(2-bromophenyl)acetonitrile

: 103317-32-4
(2-bromophenyl)thioacetamide

Guidance literature:: 2-(2-bromophenyl)acetonitrile; With Lawessons reagent; boron trifluoride diethyl etherate; In diethyl ether; toluene; at 50 ℃; for 14h; Inert atmosphere;

With sodium hydrogencarbonate; In diethyl ether; toluene; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1055/s-0028-1083253

Reference yield:

: 65999-53-3
2-(2-bromophenyl)acetamide

: 103317-32-4
(2-bromophenyl)thioacetamide

Guidance literature:: With Lawessons reagent; In tetrahydrofuran; at 80 ℃; for 12h;
DOI:10.1016/j.bmcl.2021.127846

Reference yield:

: 18698-97-0
ortho-bromophenylacetic acid

: 103317-32-4
(2-bromophenyl)thioacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2 h / 20 °C

2: ammonia / tetrahydrofuran / 12 h / 20 °C

3: Lawessons reagent / tetrahydrofuran / 12 h / 80 °C

With Lawessons reagent; oxalyl dichloride; ammonia; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.bmcl.2021.127846