C₅₂H₉₂O₈Si₃

Base Information

Chemical Name:C₅₂H₉₂O₈Si₃
CAS No.:944393-45-7
Molecular Formula:C₅₂H₉₂O₈Si₃
Molecular Weight:929.554
Hs Code.:

C<sub>52</sub>H<sub>92</sub>O<sub>8</sub>Si<sub>3</sub>

Synonyms:C₅₂H₉₂O₈Si₃

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Chemical Property of C₅₂H₉₂O₈Si₃

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Technology Process of C₅₂H₉₂O₈Si₃

There total 20 articles about C₅₂H₉₂O₈Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 944393-23-1
C₃₁H₅₄O₅Si₂

: C₅₂H₉₀O₈Si₃

: 944393-45-7
C₅₂H₉₂O₈Si₃

: epi-58

Guidance literature:: With benzo[1,3,2]dioxaborole; In tetrahydrofuran; at -78 - 0 ℃; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1055/s-0029-1216926

Reference yield:

: C₅₂H₉₀O₈Si₃

: 944393-45-7
C₅₂H₉₂O₈Si₃

: epi-58

Guidance literature:: C₅₂H₉₀O₈Si₃; With benzo[1,3,2]dioxaborole; In tetrahydrofuran; at -78 - 0 ℃;

With methanol; water; Rochelle's salt; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 19790-60-4
3-Benzyloxypropanal

: 944393-45-7
C₅₂H₉₂O₈Si₃

: epi-58

Guidance literature:: Multi-step reaction with 6 steps

1.1: borane-THF / C₁₉H₂₃NO₆S / propiononitrile / 6 h / -78 °C

1.2: pH 7

2.1: 2,6-dimethylpyridine / dichloromethane / 0 - 20 °C

3.1: pentane

3.2: 0 - 20 °C

4.1: triethylamine / dichloromethane / 1 h / 20 °C

5.1: boron trifluoride diethyl etherate / dichloromethane / -78 °C

6.1: benzo[1,3,2]dioxaborole / tetrahydrofuran / -78 - 0 °C

6.2: 20 °C

With 2,6-dimethylpyridine; borane-THF; boron trifluoride diethyl etherate; triethylamine; benzo[1,3,2]dioxaborole; C₁₉H₂₃NO₆S; In tetrahydrofuran; dichloromethane; propiononitrile; pentane;