methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

Base Information

Chemical Name:methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate
CAS No.:130145-37-8
Molecular Formula:C₁₇H₁₆N₄O₈
Molecular Weight:404.336
Hs Code.:

Synonyms:methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

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Chemical Property of methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

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Technology Process of methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

There total 3 articles about methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 130145-34-5
methyl (4-chloro-3,5-dinitrophenyl)carbamate

: 24461-61-8,26682-99-5,37760-98-8,6591-61-3
phenylglycine methyl ester

: 130145-37-8
methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

Guidance literature:: In toluene; for 23h; Heating;
DOI:10.1021/jm00173a021

Reference yield:

: 130145-33-4
4-chloro-3,5-dinitro-benzoyl azide

: 130145-37-8
methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 1.) from 20 deg C to reflux, 30 min, 2.) reflux, 2 h

2: 18 h / Ambient temperature

3: 41 percent / toluene / 23 h / Heating

In toluene;
DOI:10.1021/jm00173a021

Reference yield:

: 467443-76-1
2-Chloro-5-isocyanato-1,3-dinitro-benzene

: 130145-37-8
methyl <4-<<α-methoxycarbonyl)benzyl>amino>-3,5-dinitrophenyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: 18 h / Ambient temperature

2: 41 percent / toluene / 23 h / Heating

In toluene;
DOI:10.1021/jm00173a021