N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

Base Information

Chemical Name:N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide
CAS No.:1417038-13-1
Molecular Formula:C₁₃H₁₈N₄OS₂
Molecular Weight:310.444
Hs Code.:

Synonyms:N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

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Chemical Property of N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

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Technology Process of N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

There total 3 articles about N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,3-bis(isopropylthio)benzoyl azide

: 1417038-13-1
N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

Guidance literature:: With sodium azide; In water; at 20 - 50 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ic302149p

Reference yield:

: 85686-14-2
2,3-bis(isopropylsulfanyl)benzoic acid

: 1417038-13-1
N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / dichloromethane / 3 h / Inert atmosphere; Schlenk technique; Reflux

2: sodium azide / acetone; water / 1 h / 20 °C / Inert atmosphere; Schlenk technique

3: sodium azide / water / 2 h / 20 - 50 °C / Inert atmosphere; Schlenk technique

With thionyl chloride; sodium azide; In dichloromethane; water; acetone; 3: |Curtius Rearrangement;
DOI:10.1021/ic302149p

Reference yield:

: 911649-50-8
2,3-di(isopropylmercapto)benzoic acid chloride

: 1417038-13-1
N-{2,3-bis(isopropylthio)phenyl}carbamoyl azide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / acetone; water / 1 h / 20 °C / Inert atmosphere; Schlenk technique

2: sodium azide / water / 2 h / 20 - 50 °C / Inert atmosphere; Schlenk technique

With sodium azide; In water; acetone; 2: |Curtius Rearrangement;
DOI:10.1021/ic302149p