Cbz-ΔTrp-OMe

Base Information

Chemical Name:Cbz-ΔTrp-OMe
CAS No.:130680-69-2
Molecular Formula:C₂₀H₁₈N₂O₄
Molecular Weight:350.374
Hs Code.:

Synonyms:Cbz-ΔTrp-OMe

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Chemical Property of Cbz-ΔTrp-OMe

Chemical Property:

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Technology Process of Cbz-ΔTrp-OMe

There total 4 articles about Cbz-ΔTrp-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 130680-70-5
N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

: 130680-69-2
Cbz-ΔTrp-OMe

Guidance literature:: With lithium hydroxide; In methanol; Ambient temperature;
DOI:10.1248/cpb.38.2020

Reference yield: 30.0%

: 2717-76-2,130812-44-1,130812-46-3
(S)-N-benzyloxycarbonyl-L-tryptophan methyl ester

: 130680-69-2
Cbz-ΔTrp-OMe

Guidance literature:: With zirconium(IV) chloride; Nitrosobenzene; In toluene; at 0 - 20 ℃; for 2h;
DOI:10.1021/ja061660s

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 130680-69-2
Cbz-ΔTrp-OMe

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 1M NaOH / 1) dioxane - water, 0 deg C, 20 min, 2) r.t., 5 d

2: 1) tert-BuOK / 1) CH₂Cl₂, -70 deg C, 2) CH₂Cl₂, r.t.

3: 66 percent / 1M LiOH / methanol / Ambient temperature

With lithium hydroxide; sodium hydroxide; potassium tert-butylate; In methanol;
DOI:10.1248/cpb.38.2020