N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

Base Information

Chemical Name:N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan
CAS No.:130680-70-5
Molecular Formula:C₂₅H₂₆N₂O₆
Molecular Weight:450.491
Hs Code.:

Synonyms:N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

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Chemical Property of N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

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Technology Process of N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

There total 9 articles about N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 57476-50-3
1-tert-butoxycarbonyl-3-formylindole

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 130680-70-5
N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

: 130680-70-5
methyl (E)-3-(1-tert-butoxycarbonylindol-3-yl)-2-(carbobenzoxyamino)acrylate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 2.5h; Ambient temperature;
DOI:10.1007/BF00696717

Reference yield: 49.0%

: 57476-50-3
1-tert-butoxycarbonyl-3-formylindole

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 130680-70-5
N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

: 130680-70-5
methyl (E)-3-(1-tert-butoxycarbonylindol-3-yl)-2-(carbobenzoxyamino)acrylate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 2.5h; Ambient temperature;
DOI:10.1007/BF00696717

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 130680-70-5
N-benzyloxycarbonyl-N'-(tert-butyloxycarbonyl)-Z-α,β-didehydrotryptophan

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / K₂CO₃ / acetonitrile / 6 h / Ambient temperature

2: 49 percent / t-BuOK / tetrahydrofuran / 2.5 h / Ambient temperature

With potassium tert-butylate; potassium carbonate; In tetrahydrofuran; acetonitrile;
DOI:10.1007/BF00696717