8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene
CAS No.:1189528-64-0
Molecular Formula:C₄₇H₄₈BIN₂O₆
Molecular Weight:874.623
Hs Code.:

Synonyms:8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

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Chemical Property of 8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

There total 4 articles about 8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 31995-08-1
3-(2-methoxyethoxy)prop-1-yne

: 1189528-66-2,1260903-50-1
8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene

: 1189528-64-0
8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: 3-(2-methoxyethoxy)prop-1-yne; With ethylmagnesium bromide; In tetrahydrofuran; at 60 ℃; for 2h;

8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-difluoro-4-bora-3a,4a-diaza-s-indacene; In tetrahydrofuran; at 25 ℃; for 12h;
DOI:10.1021/cm503577y

Reference yield:

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 1189528-64-0
8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 72 h / 25 °C

1.2: 1 h

1.3: 25 °C

2.1: piperidine / toluene / 3 h / Reflux

3.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 60 °C

3.2: 12 h / 25 °C

With piperidine; ethylmagnesium bromide; In tetrahydrofuran; dichloromethane; toluene; 2.1: |Knoevenagel Condensation;
DOI:10.1021/cm503577y

Reference yield:

: 1711-02-0
4-iodobenzoic acid chloride

: 1189528-64-0
8-(4-iodophenyl)-1,7-dimethyl-3,5-bis(4-methoxystyryl)-4,4-bis(2,5-dioxaoct-7-ynyl)-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 72 h / 25 °C

1.2: 1 h

1.3: 25 °C

2.1: piperidine / toluene / 3 h / Reflux

3.1: ethylmagnesium bromide / tetrahydrofuran / 2 h / 60 °C

3.2: 12 h / 25 °C

With piperidine; ethylmagnesium bromide; In tetrahydrofuran; dichloromethane; toluene; 2.1: |Knoevenagel Condensation;
DOI:10.1021/cm503577y