(S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

Base Information

Chemical Name:(S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester
CAS No.:177469-85-1
Molecular Formula:C₂₇H₃₀N₂O₄
Molecular Weight:446.546
Hs Code.:

Synonyms:(S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

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Chemical Property of (S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

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Technology Process of (S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

There total 7 articles about (S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 931-51-1
cyclohexylmagnesiumchloride

: 177469-85-1
(S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / tetrahydrofuran / 12 h / Ambient temperature

2: 310 mg / Ph₃P, DEAD / tetrahydrofuran / 4 h / Ambient temperature

3: 70 percent / NH₂NH₂*H₂O / dioxane; ethanol / 0.5 h / Heating

4: 80 mg / AcOH / methanol; dioxane / 12 h / Ambient temperature

With hydrazine hydrate; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol;
DOI:10.1016/0957-4166(96)00340-0

Reference yield:

: 3747-74-8
2-(chloromethyl)quinoline monohydrochloride

: 177469-85-1
(S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

2: 94 percent / tetrahydrofuran / 12 h / Ambient temperature

3: 310 mg / Ph₃P, DEAD / tetrahydrofuran / 4 h / Ambient temperature

4: 70 percent / NH₂NH₂*H₂O / dioxane; ethanol / 0.5 h / Heating

5: 80 mg / AcOH / methanol; dioxane / 12 h / Ambient temperature

With potassium carbonate; hydrazine hydrate; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0957-4166(96)00340-0

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 177469-85-1
(S)-2-E-[cyclohexyl-4-(2-quinolinylmethoxy)phenyl]methoxyiminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 74 percent / K₂CO₃ / dimethylformamide / 16 h / Ambient temperature

2: 94 percent / tetrahydrofuran / 12 h / Ambient temperature

3: 310 mg / Ph₃P, DEAD / tetrahydrofuran / 4 h / Ambient temperature

4: 70 percent / NH₂NH₂*H₂O / dioxane; ethanol / 0.5 h / Heating

5: 80 mg / AcOH / methanol; dioxane / 12 h / Ambient temperature

With potassium carbonate; hydrazine hydrate; acetic acid; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0957-4166(96)00340-0