isocyanomethyl p-toluenesulfonate

Base Information

Chemical Name:isocyanomethyl p-toluenesulfonate
CAS No.:79047-38-4
Molecular Formula:C₉H₉NO₃S
Molecular Weight:211.241
Hs Code.:

Synonyms:isocyanomethyl p-toluenesulfonate

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Chemical Property of isocyanomethyl p-toluenesulfonate

Chemical Property:

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Technology Process of isocyanomethyl p-toluenesulfonate

There total 1 articles about isocyanomethyl p-toluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-(ruthenium(II)dimethylglyoximate)2(triphenylphosphine)(tosyl-methyl-isocyanide)

: 603-35-0
triphenylphosphine

: trans-(ruthenium(II)dimethylglyoximate)2(triphenylphosphine)2

: 79047-38-4
isocyanomethyl p-toluenesulfonate

Guidance literature:: In toluene; Soln. is prepared by injecting the ligand into serum-capped cell (under N2) containing the thermostated soln. of the complex.; UV-spectroscopy.; Kinetics;

Reference yield: 56.0%

: 79047-38-4
isocyanomethyl p-toluenesulfonate

: 255045-00-2
(S)-3-Benzyloxymethyl-5-oxo-octahydro-indolizine-7-carbaldehyde

: 3-benzyloxymethyl-7-(1H-imidazol-4-yl)-hexahydro-indolizin-5-one

Guidance literature:: isocyanomethyl p-toluenesulfonate; (S)-3-Benzyloxymethyl-5-oxo-octahydro-indolizine-7-carbaldehyde; With sodium cyanide; In ethanol;

With ammonia; In ethanol; at 75 ℃; for 72h;

DOI:10.1016/S0040-4039(99)01652-4

Reference yield: 53.8%

: 13755-29-8
sodium tetrafluoroborate

: [Fe(C₃₅H₃₉O₅N₄)(C₅H₅N)2]⁽²⁺⁾*Cl^(1-)*OH^(1-)=[Fe(C₃₅H₃₉O₅N₄)(C₅H₅N)2](OH)Cl

: 79047-38-4
isocyanomethyl p-toluenesulfonate

: (5-oxamesoporphyrinato IX dimethyl ester)bis(tosylmethyl isocyanide)iron(III) tetrafluoroborate hydroxide

Guidance literature:: In dichloromethane; washing a solution of the bis-pyridine complex and 50 mg of TsCH2NC in 30 ml CH2Cl2 with concd. aq. NaBF4, drying and evaporation;; chromatography (CH2Cl2-MeOH); mixture of the IXα-, IXβ-, IXγ- and IXδ-isomers obtd.; elem. anal.;;