benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate

Base Information

• Chemical Name: benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate
• CAS No.: 741699-50-3
• Molecular Formula: C₂₅H₂₆O₆S
• Molecular Weight: 454.544

Synonyms:benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate

Chemical Property of benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate

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Technology Process of benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate

There total 1 articles about benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Benzyl 4'-(2-hydroxyethoxy)-3',5'-dimethylbiphenyl-4-carboxylate (741699-32-1) + methanesulfonyl chloride (124-63-0) → benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate (741699-50-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 1h;

Reference yield:

benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate (741699-50-3) + 4-((1R,2S)-2-amino-1-hydroxypropyl)phenol (552-85-2,771-91-5,1926-72-3,13104-32-0,37692-93-6,52446-53-4,62928-85-2,62928-86-3,73027-12-0) → benzyl 4'-{2-[(1S,2R)-2-hydroxy-2-(4-hydroxyphenyl)-1-methylethylamino]ethoxy}-3',5'-dimethylbiphenyl-4-carboxylate

Guidance literature:

With diisopropylamine; In DMF (N,N-dimethyl-formamide); at 80 ℃;

Reference yield:

benzyl 4'-(2-methanesulfonyloxy-ethoxy)-3',5'-dimethylbiphenyl-4-carboxylate (741699-50-3) + N-{5-[(1R,2S)-2-Amino-1-hydroxypropyl]-2-benzyloxyphenyl}-methanesulfonamide (851334-17-3) → Benzyl 4'-{2-[(1S,2R)-2-(4-benzyloxy-3-methanesulfonyl-aminophenyl)-2-hydroxy-1-methylethylamino]ethoxy}-3',5'-dimethylbiphenyl-4-carboxylate (851336-36-2)

Guidance literature:

With diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃;

upstream raw materials:

Benzyl 4'-(2-hydroxyethoxy)-3',5'-dimethylbiphenyl-4-carboxylate

methanesulfonyl chloride

Downstream raw materials:

Benzyl 4'-{2-[(1S,2R)-2-(4-benzyloxy-3-methanesulfonyl-aminophenyl)-2-hydroxy-1-methylethylamino]ethoxy}-3',5'-dimethylbiphenyl-4-carboxylate

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