HCCC₆H₄O(CH₂)6SAc

Base Information

Chemical Name:HCCC₆H₄O(CH₂)6SAc
CAS No.:1338595-63-3
Molecular Formula:C₁₆H₂₀O₂S
Molecular Weight:276.4
Hs Code.:

HCCC<sub>6</sub>H<sub>4</sub>O(CH<sub>2</sub>)6SAc

Synonyms:HCCC₆H₄O(CH₂)6SAc

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Chemical Property of HCCC₆H₄O(CH₂)6SAc

Chemical Property:

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Technology Process of HCCC₆H₄O(CH₂)6SAc

There total 5 articles about HCCC₆H₄O(CH₂)6SAc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1338595-65-5
C₁₉H₂₈O₂SSi

: 1338595-63-3
HCCC₆H₄O(CH₂)6SAc

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1.5h;
DOI:10.1039/c1nj20235a

Reference yield:

: 1338595-64-4
I-C₆H₄-O-(CH₂)6-SAc

: 1338595-63-3
HCCC₆H₄O(CH₂)6SAc

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 72 h / 45 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1: Sonogashira coupling;
DOI:10.1039/c1nj20235a

Reference yield:

: 540-38-5
p-Iodophenol

: 1338595-63-3
HCCC₆H₄O(CH₂)6SAc

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl-formamide

2: acetone / 40 h / 20 °C

3: copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 72 h / 45 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 1.5 h / 20 °C

With copper(l) iodide; trans-bis(triphenylphosphine)palladium dichloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetone; 3: Sonogashira coupling;
DOI:10.1039/c1nj20235a