1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

Base Information

Chemical Name:1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride
CAS No.:97352-05-1
Molecular Formula:C₂₁H₂₇NO₂*ClH
Molecular Weight:361.912
Hs Code.:

Synonyms:1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

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Chemical Property of 1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

Chemical Property:

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Technology Process of 1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

There total 6 articles about 1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 84865-81-6
(5,6-dimethoxy-1,2,3,4-tetrahydronaphthalen-1-yl)methanamine hydrochloride

: 97352-05-1
1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

Guidance literature:: With hydrogen; sodium acetate; platinum on activated charcoal; In methanol; for 1h; Ambient temperature;
DOI:10.1021/jm00148a005

Reference yield:

: 24039-89-2
5,6-dimethoxy-1-tetralone

: 97352-05-1
1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: ZnI₂ / benzene / 5 h / 60 °C

2: LiAlH₄ / benzene; diethyl ether / 2 h / Heating

3: 92 percent / H₂, 12 N aq. HCl / 10percent Pd/C / methanol / 20 h / Ambient temperature

4: 92 percent / H₂, NaOAc*3H₂O / 5percent Pt/C / methanol / 1 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium acetate; zinc(II) iodide; palladium on activated charcoal; platinum on activated charcoal; In methanol; diethyl ether; benzene;
DOI:10.1021/jm00148a005

Reference yield:

: 5,6-Dimethoxy-1-trimethylsilanyloxy-1,2,3,4-tetrahydro-naphthalene-1-carbonitrile

: 97352-05-1
1-<(N-benzyl-N-methylamino)methyl>-5,6-dimethoxytetralin hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / benzene; diethyl ether / 2 h / Heating

2: 92 percent / H₂, 12 N aq. HCl / 10percent Pd/C / methanol / 20 h / Ambient temperature

3: 92 percent / H₂, NaOAc*3H₂O / 5percent Pt/C / methanol / 1 h / Ambient temperature

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen; sodium acetate; palladium on activated charcoal; platinum on activated charcoal; In methanol; diethyl ether; benzene;
DOI:10.1021/jm00148a005