N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

Base Information

Chemical Name:N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride
CAS No.:1039764-75-4
Molecular Formula:C₁₅H₁₄BrClN₂*ClH
Molecular Weight:374.107
Hs Code.:

Synonyms:N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

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Chemical Property of N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

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Technology Process of N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

There total 1 articles about N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 2856-63-5
2-Chlorophenylacetonitrile

: 5465-63-4
2-bromobenzylamine hydrochloride

: 1039764-75-4
N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

Guidance literature:: 2-bromobenzylamine hydrochloride; With trimethylaluminum; In toluene; for 2h;

2-Chlorophenylacetonitrile; In toluene; at 80 ℃; for 2h;

Reference yield: 30.0%

: 1039764-75-4
N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

: 105-53-3
diethyl malonate

: 3-[(2-bromophenyl)methyl]-2-[(2-chlorophenyl)methyl]-6-hydroxy-4(3H)-pyrimidinone

Guidance literature:: With sodium ethanolate; In ethanol; 2-methoxy-ethanol; for 24h; Heating / reflux;

Reference yield:

: 1039764-75-4
N-[(2-bromophenyl)methyl]-2-(2-chlorophenyl)ethanimidamide hydrochloride

: N-({1-[(2-bromophenyl)methyl]-2-[(2-chlorophenyl)methyl]-4-hydroxy-6-oxo-1,6-dihydro-5-pyrimidinyl}carbonyl)glycine

Guidance literature:: Multi-step reaction with 3 steps

1: sodium ethanolate / ethanol; 2-methoxy-ethanol / 24 h / Heating / reflux

2: N-ethyl-N,N-diisopropylamine / chloroform / 1.33 h / 120 °C / Microwave irradiation

3: sodium hydroxide; ethanol; water / 2 h

With sodium hydroxide; ethanol; water; sodium ethanolate; N-ethyl-N,N-diisopropylamine; In ethanol; chloroform; 2-methoxy-ethanol;