1-Methyl-4-ethyl 2-phenylsuccinate

Base Information

Chemical Name:1-Methyl-4-ethyl 2-phenylsuccinate
CAS No.:132545-36-9
Molecular Formula:C₁₃H₁₆O₄
Molecular Weight:236.268
Hs Code.:

Synonyms:1-Methyl-4-ethyl 2-phenylsuccinate

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Chemical Property of 1-Methyl-4-ethyl 2-phenylsuccinate

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Technology Process of 1-Methyl-4-ethyl 2-phenylsuccinate

There total 11 articles about 1-Methyl-4-ethyl 2-phenylsuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: (E)-2-Fluoro-3-phenyl-but-2-enedioic acid 1-ethyl ester 4-methyl ester

: 1-ethyl 4-methyl 2-fluoro-3-phenylsuccinate

: 132545-36-9
1-Methyl-4-ethyl 2-phenylsuccinate

Guidance literature:: With C₃₆H₄₉IrN₂OP⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); hydrogen; In toluene; at 20 ℃; for 24h; under 75007.5 Torr; stereoselective reaction; Inert atmosphere; High pressure;
DOI:10.1021/jacs.8b08778

Reference yield: 57.0%

: 132545-38-1
(E)-4-ethyl 1-methyl 2-phenylfumarate

: 132545-36-9
1-Methyl-4-ethyl 2-phenylsuccinate

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethanol;
DOI:10.1002/anie.202107982

Reference yield:

: 22979-35-7
Methyl phenyldiazoacetate

: 132545-36-9
1-Methyl-4-ethyl 2-phenylsuccinate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium bromide; dirhodium cofactor covalently linked to prolyl oligopeptidase scaffold containing a genetically encoded azidophenylalanine (Z) residue at position 477 mutant 5-G / tetrahydrofuran / 22 h / 4 °C / pH 7.4 / Enzymatic reaction

2: palladium on activated charcoal; hydrogen / ethanol

With palladium on activated charcoal; hydrogen; dirhodium cofactor covalently linked to prolyl oligopeptidase scaffold containing a genetically encoded azidophenylalanine (Z) residue at position 477 mutant 5-G; sodium bromide; In tetrahydrofuran; ethanol;
DOI:10.1002/anie.202107982