ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate

Base Information

Chemical Name:ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate
CAS No.:1278521-24-6
Molecular Formula:C₂₂H₂₁Cl₂NO₃S
Molecular Weight:450.386
Hs Code.:

Synonyms:ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate

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Chemical Property of ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate

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Technology Process of ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate

There total 2 articles about ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1273326-22-9
C₁₁H₈Cl₂S

: 124156-21-4
ethyl (4-methoxyphenylimino)acetate

: 1278521-24-6
ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate

Guidance literature:: With iron(III) chloride hexahydrate; In nitromethane; toluene; at 20 ℃; for 48h; regioselective reaction;
DOI:10.1016/j.tet.2011.01.039

Reference yield:

: 104-94-9
4-methoxy-aniline

: 1278521-24-6
ethyl (4-methoxyphenylamino)(5-(2,4-dichlorobenzyl)thiophen-2-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 0.5 h / Molecular sieve; Sonication

2: iron(III) chloride hexahydrate / nitromethane; toluene / 48 h / 20 °C

With iron(III) chloride hexahydrate; In nitromethane; dichloromethane; toluene; 2: Friedel Crafts alkylation;
DOI:10.1016/j.tet.2011.01.039