C₁₉H₂₆O₄Si

Base Information

Chemical Name:C₁₉H₂₆O₄Si
CAS No.:1353720-78-1
Molecular Formula:C₁₉H₂₆O₄Si
Molecular Weight:346.499
Hs Code.:

C<sub>19</sub>H<sub>26</sub>O<sub>4</sub>Si

Synonyms:C₁₉H₂₆O₄Si

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Chemical Property of C₁₉H₂₆O₄Si

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Technology Process of C₁₉H₂₆O₄Si

There total 1 articles about C₁₉H₂₆O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 191427-03-9
(S)-2-phenyl-2,3-dihydrofuran

: 379224-67-6
trimethylsilylethynylglyoxylic acid ethyl ester

: 1353720-78-1
C₁₉H₂₆O₄Si

Guidance literature:: (S)-2-phenyl-2,3-dihydrofuran; trimethylsilylethynylglyoxylic acid ethyl ester; With titanium tetrachloride; In dichloromethane; at -78 ℃; for 1.5h; Inert atmosphere;

With triethylsilane; In dichloromethane; acetonitrile; at 20 ℃; for 3h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol203093g

Reference yield:

: 1353720-78-1
C₁₉H₂₆O₄Si

: C₁₆H₂₀O₆

Guidance literature:: C₁₉H₂₆O₄Si; With borane-THF; In tetrahydrofuran; at 0 ℃; for 3h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In tetrahydrofuran; water; at 50 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol203093g

Reference yield:

: 1353720-78-1
C₁₉H₂₆O₄Si

: C₁₄H₁₆O₆

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

1.2: 12 h / 50 °C / Inert atmosphere

2.1: water; lithium hydroxide / tetrahydrofuran; methanol / 6 h / Inert atmosphere

With borane-THF; water; lithium hydroxide; In tetrahydrofuran; methanol; 1.1: Hydroboration reaction;
DOI:10.1021/ol203093g