4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

Base Information

Chemical Name:4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester
CAS No.:252264-88-3
Molecular Formula:C₁₇H₂₂O₃
Molecular Weight:274.36
Hs Code.:

Synonyms:4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

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Chemical Property of 4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

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Technology Process of 4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

There total 13 articles about 4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 407-25-0
trifluoroacetic anhydride

: 252264-87-2
6-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-(ethoxycarbonyl)-3,5-hexadienoic acid

: 252264-88-3
4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

Guidance literature:: trifluoroacetic anhydride; 6-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-(ethoxycarbonyl)-3,5-hexadienoic acid; With triethylamine; In tetrahydrofuran; at 2 ℃; for 20h;

With sodium tetrahydroborate; In ethanol; at 0 ℃; for 1h;
DOI:10.1021/jo9909148

Reference yield:

: 407-25-0
trifluoroacetic anhydride

: 252264-87-2
6-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-(ethoxycarbonyl)-3,5-hexadienoic acid

: 252264-88-3
4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

: 3-(2,2,2-Trifluoro-acetoxy)-4-((R)-1,2,2-trimethyl-cyclopent-3-enyl)-benzoic acid ethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; at 2 ℃; for 20h;
DOI:10.1021/jo9909148

Reference yield:

: 541-41-3
chloroformic acid ethyl ester

: 252264-87-2
6-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-(ethoxycarbonyl)-3,5-hexadienoic acid

: 252264-88-3
4-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-hydroxybenzoic acid ethyl ester

: 2-[(E)-3-((S)-1,2,2-Trimethyl-cyclopent-3-enyl)-prop-2-en-(E)-ylidene]-succinic acid diethyl ester

Guidance literature:: chloroformic acid ethyl ester; 6-[(1R)-1,2,2-trimethylcyclopent-3-enyl]-3-(ethoxycarbonyl)-3,5-hexadienoic acid; With triethylamine; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With sodium hydroxide; In ethanol; at 20 ℃; for 0.166667h;
DOI:10.1021/jo9909148