a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

Base Information

Chemical Name:a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride
CAS No.:1449650-86-5
Molecular Formula:C₁₈H₂₂N₂*ClH
Molecular Weight:302.847
Hs Code.:

a-amino-3-phenyl-1-tricyclo[3.3.1.1<sup>3,7</sup>]decaneacetonitrile hydrochloride

Synonyms:a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

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Chemical Property of a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

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Technology Process of a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

There total 2 articles about a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 7677-24-9
trimethylsilyl cyanide

: 29835-32-3
3-phenyl-1-tricyclo[3.3.1.1^3,7]decanecarboxaldehyde

: 1449650-86-5
a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

Guidance literature:: trimethylsilyl cyanide; 3-phenyl-1-tricyclo[3.3.1.1^3,7]decanecarboxaldehyde; With zinc(II) iodide;

With ammonia; In methanol; chloroform; at 70 - 75 ℃; for 20h; Sealed tube;
DOI:10.1039/c3md00081h

Reference yield:

: 37589-22-3
3-phenyl-adamantane-1-carboxylic acid

: 1449650-86-5
a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridinium chlorochromate / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2.1: zinc(II) iodide

2.2: 20 h / 70 - 75 °C / Sealed tube

With pyridinium chlorochromate; zinc(II) iodide; In dichloromethane; 2.1: |Strecker Aminoacid Synthesis / 2.2: |Strecker Aminoacid Synthesis;
DOI:10.1039/c3md00081h

Reference yield: 100.0%

: 1449650-86-5
a-amino-3-phenyl-1-tricyclo[3.3.1.1^3,7]decaneacetonitrile hydrochloride

: 1-(3-cyclohexyl-1-tricyclo[3.3.1.1^3,7]decyl)-1,2-ethanediamine dihydrochloride

Guidance literature:: With hydrogenchloride; platinum(IV) oxide; hydrogen; In methanol; ethanol; at 60 ℃; for 8h; under 2844.39 Torr;
DOI:10.1039/c3md00081h