L-isoleucyl-L-cyclohexylglycine methyl amide

Base Information

Chemical Name:L-isoleucyl-L-cyclohexylglycine methyl amide
CAS No.:871917-45-2
Molecular Formula:C₁₅H₂₉N₃O₂
Molecular Weight:283.414
Hs Code.:

Synonyms:L-isoleucyl-L-cyclohexylglycine methyl amide

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Chemical Property of L-isoleucyl-L-cyclohexylglycine methyl amide

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Technology Process of L-isoleucyl-L-cyclohexylglycine methyl amide

There total 4 articles about L-isoleucyl-L-cyclohexylglycine methyl amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: {(1S,2S)-1-[((S)-Cyclohexyl-methylcarbamoyl-methyl)-carbamoyl]-2-methyl-butyl}-carbamic acid tert-butyl ester

: 871917-45-2
L-isoleucyl-L-cyclohexylglycine methyl amide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.666667h;
DOI:10.1021/jo0517848

Reference yield:

: 862118-89-6
tert-butyl (S)-(1-cyclohexyl-2-(methylamino)-2-oxoethyl)carbamate

: 871917-45-2
L-isoleucyl-L-cyclohexylglycine methyl amide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 440 mg / trifluoroacetic acid / CH₂Cl₂ / 0.67 h / 20 °C

2.1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; HOBt / CH₂Cl₂ / 0.5 h / 0 °C

2.2: CH₂Cl₂

3.1: 69 mg / trifluoroacetic acid / CH₂Cl₂ / 0.67 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo0517848

Reference yield:

: 109183-71-3
N-(tert-butoxycarbonyl)-L-cyclohexylglycine

: 871917-45-2
L-isoleucyl-L-cyclohexylglycine methyl amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; HOBt / CH₂Cl₂ / 0.5 h / 0 °C

1.2: CH₂Cl₂; methanol

2.1: 440 mg / trifluoroacetic acid / CH₂Cl₂ / 0.67 h / 20 °C

3.1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; HOBt / CH₂Cl₂ / 0.5 h / 0 °C

3.2: CH₂Cl₂

4.1: 69 mg / trifluoroacetic acid / CH₂Cl₂ / 0.67 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo0517848