L-cyclohexylglycine-N-methylamide

Base Information

Chemical Name:L-cyclohexylglycine-N-methylamide
CAS No.:188728-68-9
Molecular Formula:C₉H₁₈N₂O
Molecular Weight:170.255
Hs Code.:

Synonyms:L-cyclohexylglycine-N-methylamide

Suppliers and Price of L-cyclohexylglycine-N-methylamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of L-cyclohexylglycine-N-methylamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of L-cyclohexylglycine-N-methylamide

There total 3 articles about L-cyclohexylglycine-N-methylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 862118-89-6
tert-butyl (S)-(1-cyclohexyl-2-(methylamino)-2-oxoethyl)carbamate

: 188728-68-9
L-cyclohexylglycine-N-methylamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.666667h;
DOI:10.1021/jo0517848

Reference yield:

: 109183-71-3
N-(tert-butoxycarbonyl)-L-cyclohexylglycine

: 188728-68-9
L-cyclohexylglycine-N-methylamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide hydrochloride; HOBt / CH₂Cl₂ / 0.5 h / 0 °C

1.2: CH₂Cl₂; methanol

2.1: 440 mg / trifluoroacetic acid / CH₂Cl₂ / 0.67 h / 20 °C

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo0517848

Reference yield:

: 129213-83-8
(S)-2-amino-N-methyl-2-phenylacetamide

: 188728-68-9
L-cyclohexylglycine-N-methylamide

Guidance literature:: With sodium tetrahydroborate; rhodium(III) chloride; Yield given; Multistep reaction; 1.) EtOH, 30 deg C, 2 h, 2.) EtOH, RT, 4 h;
DOI:10.1021/jm970404a