3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

Base Information

Chemical Name:3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole
CAS No.:618430-04-9
Molecular Formula:C₁₅H₁₁Cl₂N₃OS
Molecular Weight:352.244
Hs Code.:

3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4<i>H</i>-[1,2,4]triazole

Synonyms:3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

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Chemical Property of 3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

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Technology Process of 3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

There total 3 articles about 3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 618430-01-6
5-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-2,4-dihydro-[1,2,4]triazole-3-thione

: 74-88-4
methyl iodide

: 618430-04-9
3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

Guidance literature:: With sodium hydroxide; In ethanol; water; for 0.05h; sonication;
DOI:10.1016/S0968-0896(02)00469-8

Reference yield:

: 618430-15-2
4-chloro-2-(2-chlorophenoxy)benzoic acid chloride

: 618430-04-9
3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / benzene / -5 - 20 °C

1.2: 84 percent / NaOH / H₂O / 8 h / Heating

2.1: 87 percent / NaOH / H₂O; ethanol / 0.05 h / sonication

With pyridine; sodium hydroxide; In ethanol; water; benzene;
DOI:10.1016/S0968-0896(02)00469-8

Reference yield:

: 69199-99-1
4-chloro-2-(2-chlorophenoxy)benzoic acid

: 618430-04-9
3-[4-chloro-2-(2-chloro-phenoxy)-phenyl]-5-methylsulfanyl-4H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 3 steps

1.1: SOCl₂ / 50 - 55 °C

2.1: pyridine / benzene / -5 - 20 °C

2.2: 84 percent / NaOH / H₂O / 8 h / Heating

3.1: 87 percent / NaOH / H₂O; ethanol / 0.05 h / sonication

With pyridine; sodium hydroxide; thionyl chloride; In ethanol; water; benzene;
DOI:10.1016/S0968-0896(02)00469-8