propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

Base Information

Chemical Name:propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester
CAS No.:1154062-15-3
Molecular Formula:C₂₂H₂₆O₆
Molecular Weight:386.445
Hs Code.:

Synonyms:propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

Suppliers and Price of propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

There total 1 articles about propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 916525-75-2
(1R,2S)-1-(2-methoxyethoxy)-1,2-bis-(2-methoxyphenyl)-ethanol

: 814-68-6,25189-84-8
acryloyl chloride

: 1154062-15-3
propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.004

Reference yield:

: 1154062-15-3
propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: exo-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

: 120-74-1,934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7
(1S,2S,4S)-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

: 58001-99-3
5-norbornene-2-carboxylic acid

Guidance literature:: propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester; With dimethyl aluminium chloride; In tetrahydrofuran; at -80 ℃; for 0.0166667h; Inert atmosphere;

cyclopenta-1,3-diene; In tetrahydrofuran; at -80 ℃; for 2.5h; optical yield given as %ee; Further stages; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.004

Reference yield:

: 1154062-15-3
propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-diphenylethyl ester

: 1154062-19-7
bicyclo[2.2.1]hept-5-ene-2-carboxylic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-diphenylethyl ester

Guidance literature:: propenoic acid (1R,2S)-2-(2-methoxyethoxy)-1,2-bis(2-methoxyphenyl)ethyl ester; With dimethyl aluminium chloride; In tetrahydrofuran; at -80 ℃; for 0.0166667h; Inert atmosphere;

cyclopenta-1,3-diene; In tetrahydrofuran; at -80 - -50 ℃; for 2.5h; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.004