3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

Base Information

• Chemical Name: 3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide
• CAS No.: 1246677-08-6
• Molecular Formula: C₄₉H₇₅N₇O₁₅S
• Molecular Weight: 1034.24

Synonyms:3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

Chemical Property of 3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

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Technology Process of 3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

There total 1 articles about 3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide (1246677-06-4) + Boc-Lys(Boc)-OH (2483-46-7) → 5'-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide (1246677-07-5) + 3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide (1246677-08-6)

Guidance literature:

With dmap; benzotriazol-1-ol; triethylamine; diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1039/c0cc00645a

Reference yield: 85.0%

3',5'-di-(N-α,ω-di-Boc-L-lysyl)-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide (1246677-08-6) → 3',5'-di-L-lysyl-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide (1246677-16-6)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

DOI:10.1039/c0cc00645a

upstream raw materials:

C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

Boc-Lys(Boc)-OH

Downstream raw materials:

3',5'-di-L-lysyl-C-(2'-deoxy-α-D-ribofuranosyl-1')-N-[3-(2-acetylaminothiazole-4-yl)phenyl]carboxamide

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