methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

Base Information

Chemical Name:methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate
CAS No.:956467-98-4
Molecular Formula:C₁₉H₂₈N₂O₅
Molecular Weight:364.442
Hs Code.:

Synonyms:methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

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Chemical Property of methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

Chemical Property:

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Technology Process of methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

There total 1 articles about methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15761-38-3
L-N-Boc-Ala

: 95071-12-8
(S)-N-benzyl-1-methoxy-1-oxopropan-2-aminium chloride

: 956467-98-4
methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 956467-98-4
methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

: 956467-99-5
(3S,6S)-4-benzyl-3,6-dimethylpiperazine-2,5-dione

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield:

: 956467-98-4
methyl N-{[(1,1-dimethylethyl)oxy]carbonyl}-L-alanyl-N-(phenylmethyl)-L-alaninate

: 956467-53-1
(2S,5S)-1-{[3,4-bis(methyloxy)phenyl]sulfonyl}-4-{[3-fluoro-4-(methyloxy)phenyl]sulfonyl}-2,5-dimethylpiperazine

Guidance literature:: Multi-step reaction with 5 steps

1: trifluoroacetic acid / dichloromethane / 0.5 h / 20 °C

2: borane-THF / tetrahydrofuran / 7 h / Heating / reflux

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

4: hydrogenchloride; water; hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 72 h / 20 °C

With hydrogenchloride; borane-THF; water; hydrogen; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; dichloromethane;