3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

Base Information

Chemical Name:3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone
CAS No.:116490-92-7
Molecular Formula:C₂₅H₂₈N₄O₇
Molecular Weight:496.52
Hs Code.:

Synonyms:3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

Suppliers and Price of 3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

Chemical Property:

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Technology Process of 3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

There total 4 articles about 3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 80496-84-0
3,4,5-tri-O-acetyl-L-erythro-pentosulose 1,2-bis(phenylhydrazone)

: 75-36-5
acetyl chloride

: 101996-76-3,116490-92-7
Acetic acid (R)-3-(acetyl-phenyl-hydrazono)-1-((S)-1,2-diacetoxy-ethyl)-2-(phenyl-hydrazono)-propyl ester

Guidance literature:: With N,N-dimethyl-aniline;
DOI:10.1016/S0008-6215(00)90424-5

Reference yield: 70.0%

: 4092-28-8
Tri-O-acetyl-D-erythro-pentose-phenylosazon

: 75-36-5
acetyl chloride

: 116490-92-7
3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

Guidance literature:: In various solvent(s); for 19h; Ambient temperature;
DOI:10.1016/0008-6215(88)84141-7

Reference yield:

: 3322-01-8
D-erythropentose phenylosazone

: 116490-92-7
3,4,5-tri-O-acetyl-D-erythro-pentosulose 1-acetylphenylhydrazone 2-phenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / pyridine / 15 h / Ambient temperature

2: 70 percent / various solvent(s) / 19 h / Ambient temperature

In pyridine;
DOI:10.1016/0008-6215(88)84141-7