dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate

Base Information

Chemical Name:dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate
CAS No.:180294-98-8
Molecular Formula:C₁₂H₂₀NO₆P
Molecular Weight:305.268
Hs Code.:

Synonyms:dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate

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Chemical Property of dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate

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Technology Process of dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate

There total 2 articles about dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 180294-88-6
dimethyl {3-[(tert-butoxycarbonyl)(tert-butoxycarbonyloxy)amino]-1-cyclohexen-1-yl}phosphonate

: 180294-98-8
dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 6 h / Ambient temperature

2: 1.) NaHCO₃, 2.) pyridine / 1.) CH₂Cl₂, room temperature, 2.5 h, 2.) CH₂Cl₂, room temperature, 16 h

With pyridine; sodium hydrogencarbonate; In dichloromethane;
DOI:10.1080/10426509608046350

Reference yield:

: 108-24-7
acetic anhydride

: (3-Hydroxyamino-cyclohex-1-enyl)-phosphonic acid dimethyl ester; compound with trifluoro-acetic acid

: 180294-98-8
dimethyl {[3-(N-acetyl-N-acetyloxy)amino]-1-cyclohexen-1-yl}phosphonate

Guidance literature:: With pyridine; sodium hydrogencarbonate; Yield given. Multistep reaction; 1.) CH₂Cl₂, room temperature, 2.5 h, 2.) CH₂Cl₂, room temperature, 16 h;
DOI:10.1080/10426509608046350