2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol

Base Information

Chemical Name:2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol
CAS No.:1012319-40-2
Molecular Formula:C₂₃H₄₀O₃Si
Molecular Weight:392.654
Hs Code.:

Synonyms:2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol

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Technology Process of 2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol

There total 1 articles about 2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1012319-26-4
[1-(2-benzyloxy-ethyl)-hex-5-enyloxy]-tert-butyl-dimethyl-silane

: 141-78-6
ethyl acetate

: 1012319-40-2
2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol

Guidance literature:: With titanium(IV)isopropoxide; cyclohexylmagnesium bromide; In tetrahydrofuran; at 20 - 25 ℃; Inert atmosphere;
DOI:10.1021/ol702955m

Reference yield: 79.0%

: 1012319-40-2
2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol

: 10-benzyloxy-8-(tert-butyl-dimethyl-silanyloxy)-dec-3-en-2-one

Guidance literature:: 2-[6-benzyloxy-4-(tert-butyl-dimethyl-silanyloxy)-hexyl]-1-methyl-cyclopropanol; With N-chloro-succinimide; ferric nitrate; In N,N-dimethyl-formamide; at 0 ℃; Inert atmosphere;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol702955m