ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

Base Information

Chemical Name:ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate
CAS No.:722549-31-7
Molecular Formula:C₁₆H₁₅Cl₂NO₃S
Molecular Weight:372.272
Hs Code.:

Synonyms:ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

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Chemical Property of ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

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Technology Process of ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

There total 4 articles about ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 722549-29-3
3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-ethoxy-5-oxopentanoic acid

: 722549-31-7
ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

Guidance literature:: With oxalyl dichloride; In dichloromethane;
DOI:10.1016/j.bmcl.2005.11.017

Reference yield:

: 722549-30-6
4-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]dihydro-2H-pyran-2,6-(3H)-dione

: 722549-31-7
ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: Heating

2: oxalyl chloride / CH₂Cl₂

With oxalyl dichloride; In dichloromethane;
DOI:10.1016/j.bmcl.2005.11.017

Reference yield:

: 3-[2-(4-chloro-phenyl)-thiazol-5-yl]-pentanedioic acid

: 722549-31-7
ethyl 5-chloro-3-[2-(4-chlorophenyl)-1,3-thiazol-5-yl]-5-oxopentanoate

Guidance literature:: Multi-step reaction with 3 steps

1: Ac₂O / Heating

2: Heating

3: oxalyl chloride / CH₂Cl₂

With oxalyl dichloride; acetic anhydride; In dichloromethane;
DOI:10.1016/j.bmcl.2005.11.017