4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

Base Information

Chemical Name:4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate
CAS No.:884511-70-0
Molecular Formula:C₂₃H₃₇N₃O₆Si
Molecular Weight:479.649
Hs Code.:

Synonyms:4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

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Chemical Property of 4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

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Technology Process of 4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

There total 6 articles about 4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 884511-14-2
(S)-2-(trimethylsilyl)ethyl 2-amino-3-cyclohexylpropyl(methyl)carbamate

: 7693-46-1
4-Nitrophenyl chloroformate

: 884511-70-0
4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃;
DOI:10.1016/j.bmcl.2009.04.140 DOI:10.1016/j.bmcl.2009.11.066

Reference yield:

: 884511-15-3
(S)-tert-butyl 1-cyclohexyl-3-(methylamino)propan-2-ylcarbamate

: 884511-70-0
4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / water; acetone / 1.5 h / 0 - 20 °C

2: toluene-4-sulfonic acid / diethyl ether; ethanol; water / 0.5 h / 60 - 65 °C

3: pyridine / dichloromethane / 0.08 h / 20 °C

With pyridine; potassium carbonate; toluene-4-sulfonic acid; In diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2011.06.043

Reference yield:

: 884511-16-4
(S)-tert-butyl 1-cyclohexyl-3-(N-methyl-N-(2-(trimethylsilyl)ethoxycarbonyl)amino)propan-2-ylcarbamate

: 884511-70-0
4-nitrophenyl (S)-(3-cyclohexyl-1-((2-(trimethylsilyl)ethylcarbamate)methylamino)propan-2-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / diethyl ether; ethanol; water / 0.5 h / 60 - 65 °C

2: pyridine / dichloromethane / 0.08 h / 20 °C

With pyridine; toluene-4-sulfonic acid; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1016/j.bmcl.2011.06.043