1-cyclohexanol

Base Information

Chemical Name:1-cyclohexanol
CAS No.:175656-41-4
Molecular Formula:C₁₅H₂₂O₃S
Molecular Weight:282.404
Hs Code.:

1-<Methoxy(4-methoxyphenylsulfanyl)methyl>cyclohexanol

Synonyms:1-cyclohexanol

Suppliers and Price of 1-cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-cyclohexanol

Chemical Property:

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Technology Process of 1-cyclohexanol

There total 1 articles about 1-cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 90673-67-9
(4-methoxyphenylthio)methyl methyl ether

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 175656-41-4
1-cyclohexanol

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -45 to -28 deg C, 25 min, 2.) -20 deg C, 30 min;
DOI:10.1039/p19960000359

Reference yield: 87.0%

: 175656-41-4
1-cyclohexanol

: 175656-40-3
1-(4-Methoxyphenylsulfanyl)cyclohexanecarbaldehyde

Guidance literature:: With thionyl chloride; triethylamine; In dichloromethane; at -5 - -2 ℃; for 1h;
DOI:10.1039/p19960000359

Reference yield:

: 175656-41-4
1-cyclohexanol

: (1RS,2RS)-1-<1-(4-Methoxyphenylsulfanyl)cyclohexyl>-2-methylpropane-1,3-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / SOCl₂, Et₃N / CH₂Cl₂ / 1 h / -5 - -2 °C

2: 30 percent / LDA / tetrahydrofuran; hexane / 0.22 h / -78 - -45 °C

3: LiAlH₄ / tetrahydrofuran / 1.75 h / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1039/p19960000359