N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide

Base Information

• Chemical Name: N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide
• CAS No.: 161038-40-0
• Molecular Formula: C₁₈H₁₅N₅O₄
• Molecular Weight: 365.348

Synonyms:N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide

Chemical Property of N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide

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Technology Process of N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide

There total 1 articles about N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-<1-(carbazoylmethyl)-1,2,5,6,7,8-hexahydro-5-hydrazono-2-oxo-3-quinolinyl>benzamide (161038-39-7) → N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide (161038-40-0)

Guidance literature:

With hydrogenchloride; sodium nitrite; at 0 ℃; for 0.0833333h;

DOI:10.1002/jhet.5570310601

Reference yield: 100.0%

N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide (161038-40-0) → N-<1,2,5,6,7,8-hexahydro-1-(isocyanatomethyl)-2,5-dioxo-3-quinolinyl>benzamide (161038-42-2)

Guidance literature:

at 98 - 100 ℃; for 0.166667h;

DOI:10.1002/jhet.5570310601

Reference yield: 77.0%

N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide (161038-40-0) → N-(1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl)benzamide (161038-43-3) + 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetic acid (161038-37-5)

Guidance literature:

With potassium hydroxide; at 0 ℃; for 30h;

DOI:10.1002/jhet.5570310601

upstream raw materials:

N-<1-(carbazoylmethyl)-1,2,5,6,7,8-hexahydro-5-hydrazono-2-oxo-3-quinolinyl>benzamide

Downstream raw materials:

methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

N-(1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl)benzamide

3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetic acid

N-<1,2,5,6,7,8-hexahydro-1-(isocyanatomethyl)-2,5-dioxo-3-quinolinyl>benzamide

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