methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

Base Information

Chemical Name:methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate
CAS No.:161038-38-6
Molecular Formula:C₁₉H₁₈N₂O₅
Molecular Weight:354.362
Hs Code.:

Synonyms:methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

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Chemical Property of methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

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Technology Process of methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

There total 4 articles about methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 67-56-1
methanol

: 161038-40-0
N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide

: 161038-38-6
methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

Guidance literature:: With triethylamine; for 1h; Ambient temperature;
DOI:10.1002/jhet.5570310601

Reference yield:

: 92856-34-3
3-benzoylamino-5-oxo-5,6,7,8-tetrahydrocoumarin

: 161038-38-6
methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / dimethylformamide / 0.42 h / Heating

2: HCl / Ambient temperature

With hydrogenchloride; sodium methylate; In N,N-dimethyl-formamide;
DOI:10.1002/jhet.5570310601

Reference yield:

: 161038-40-0
N-<1-<(azidocarbonyl)methyl>-1,2,5,6,7,8-hexahydro-2,5-dioxo-3-quinolinyl>benzamide

: 161038-38-6
methyl 3-(benzoylamino)-5,6,7,8-tetrahydro-2,5-dioxo-1(2H)-quinolineacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / 5percent aq. KOH / 30 h / 0 °C

2: HCl / Ambient temperature

With hydrogenchloride; potassium hydroxide;
DOI:10.1002/jhet.5570310601