3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

Base Information

Chemical Name:3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol
CAS No.:467252-62-6
Molecular Formula:C₁₉H₃₂O₆S
Molecular Weight:388.525
Hs Code.:

Synonyms:3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

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Chemical Property of 3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

Chemical Property:

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Technology Process of 3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

There total 5 articles about 3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 130955-38-3
2,5,8,11,14-pentaoxahexadecan-16-yl methanesulfonate

: 339354-89-1
2-methyl-3-sulfanylbenzyl alcohol

: 467252-62-6
3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

Guidance literature:: With triethylamine; In acetonitrile; at 20 ℃; for 72h;
DOI:10.1021/jm0208673

Reference yield:

: 1975-50-4
2-methyl-3-nitrobenzic acid

: 467252-62-6
3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 5 steps

1.1: H₂ / Pd/C

2.1: NaNO₂; H⁺

2.2: potassium ethyl xanthogenate; aq. Na₂CO₃ / pH 8

2.3: 14.66 g / aq. NaOH / 20 h / Heating

3.1: 93 percent / H₂SO₄ / 48 h / Heating

4.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

5.1: 32 percent / Et₃N / acetonitrile / 72 h / 20 °C

With lithium aluminium tetrahydride; sulfuric acid; hydrogen; hydrogen cation; triethylamine; sodium nitrite; palladium on activated charcoal; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm0208673

Reference yield:

: 52130-17-3
3-amino-2-methylbenzoic acid

: 467252-62-6
3-{[2-(2-{2-[2-(2-methoxyethoxy)ethoxy]ethoxy}ethoxy)ethyl]sulfanyl}-2-methylbenzyl alcohol

Guidance literature:: Multi-step reaction with 4 steps

1.1: NaNO₂; H⁺

1.2: potassium ethyl xanthogenate; aq. Na₂CO₃ / pH 8

1.3: 14.66 g / aq. NaOH / 20 h / Heating

2.1: 93 percent / H₂SO₄ / 48 h / Heating

3.1: 96 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

4.1: 32 percent / Et₃N / acetonitrile / 72 h / 20 °C

With lithium aluminium tetrahydride; sulfuric acid; hydrogen cation; triethylamine; sodium nitrite; In tetrahydrofuran; acetonitrile;
DOI:10.1021/jm0208673