1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

Base Information

Chemical Name:1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone
CAS No.:1421829-27-7
Molecular Formula:C₂₀H₁₈N₂O₂S
Molecular Weight:350.441
Hs Code.:

Synonyms:1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

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Chemical Property of 1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

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Technology Process of 1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

There total 4 articles about 1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1359979-01-3
C₁₄H₁₆N₂O₂S

: 66003-76-7
Diphenyliodonium triflate

: 1421829-27-7
1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 12h; Reflux;
DOI:10.1016/j.tetlet.2012.10.131

Reference yield:

: 1359979-01-3
C₁₄H₁₆N₂O₂S

: 120976-84-3
phenyl(p-tolyl)iodonium trifluoromethanesulfonate

: 1421829-27-7
1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

: C₂₁H₂₀N₂O₂S

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 12h; Reflux;
DOI:10.1016/j.tetlet.2012.10.131

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 1421829-27-7
1-(4-(3-methoxyphenyl)-6-methyl-2-(phenylthio)pyrimidin-5-yl) ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / 24 h / 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 12 h / Reflux

With hydrogenchloride; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2012.10.131