(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

Base Information

Chemical Name:(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone
CAS No.:154052-49-0
Molecular Formula:C₁₈H₂₃NO₃S
Molecular Weight:333.452
Hs Code.:

Synonyms:(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

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Technology Process of (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

There total 1 articles about (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 2346-24-9
2-thio-2,4-oxazolidinedione

: 1620-98-0
3,5-di-t-butyl-4-hydroxybenzaldehyde

: 154052-49-0
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

Guidance literature:: With acetic acid; 3-amino propanoic acid; In toluene; for 4h; Heating;
DOI:10.1021/jm00028a017

Reference yield: 83.0%

: 154052-49-0
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

: 74-88-4
methyl iodide

: 154052-55-8
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-(methylthio)-4(5H)-oxazolone

Guidance literature:: With triethylamine; In tetrahydrofuran; for 24h;
DOI:10.1021/jm00028a017

Reference yield:

: 154052-49-0
(Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2-thioxo-4-oxazolidinone

: (Z)-5-<<3,5-bis(1,1-dimethylethyl)-4-hydroxyphenyl>methylene>-2,4-oxazolidinedione

Guidance literature:: Multi-step reaction with 2 steps

1: 83 percent / Et₃N / tetrahydrofuran / 24 h

2: 51 percent / aq. HCl / ethanol / 4 h

With hydrogenchloride; triethylamine; In tetrahydrofuran; ethanol;
DOI:10.1021/jm00028a017