5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine

Base Information

• Chemical Name: 5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine
• CAS No.: 80738-65-4
• Molecular Formula: C₅H₁₁O₄P*C₆H₁₅N
• Molecular Weight: 267.305

Synonyms:5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine

Chemical Property of 5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine

Chemical Property:

Purity/Quality:

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Technology Process of 5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine

There total 1 articles about 5,5-Dimethyl-2-oxo-2λ⁵-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.9%

Brigl's anhydride (3867-86-5,5624-44-2) + 5,5-dimethyl-1,3,2-dioxophosphorinanylselenoate (53856-23-8) → 5,5-Dimethyl-2-oxo-2λ5-[1,3,2]dioxaphosphinan-2-ol; compound with triethyl-amine (80738-65-4) + 1-1'-diselenobis<1-deoxy-2-(5,5-dimethyl-2-oxo-1,3,2-dioxaphosphorinanyloxo)-3,4,6-tri-O-acetyl-β-D-glucopyranose> (80738-68-7) + D-glucal triacetate (2873-29-2)

Guidance literature:

In benzene; at 24 ℃; for 144h;

DOI:10.1016/S0040-4020(01)98912-4

upstream raw materials:

Brigl's anhydride

5,5-dimethyl-1,3,2-dioxophosphorinanylselenoate

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