(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

Base Information

Chemical Name:(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane
CAS No.:1318115-02-4
Molecular Formula:C₂₄H₃₃NO₅
Molecular Weight:415.53
Hs Code.:

Synonyms:(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

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Chemical Property of (1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

Chemical Property:

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Technology Process of (1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

There total 1 articles about (1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 64471-47-2
(R)-α-phenyl-α-cyclopentyl-α-hydroxyacetate methyl ester

: 154905-39-2,152533-46-5,154905-36-9
(-)-exo-7-<(1,1-Domethylethoxy)carbonyl>-7-azabicyclo<2.2.1>heptan-2-ol

: 1318115-02-4
(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

Guidance literature:: With sodium hydride; In n-heptane; mineral oil; at 100 ℃; for 20h;

Reference yield:

: 1318115-02-4
(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

: 1318115-18-2
(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-methyl-7-azabicyclo[2.2.1]heptane

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

1.2: pH 10

2.1: water; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

With hydrogenchloride; water; sodium tris(acetoxy)borohydride; In 1,4-dioxane; 1,2-dichloro-ethane;

Reference yield:

: 1318115-02-4
(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7-(tert-butoxycarbonyl)-7-azabicyclo[2.2.1]heptane

: 1318114-57-6,84095-08-9
(1R,2S)-2-((R)-2'-cyclopentyl-2'-hydroxy-2'-phenylacetoxy)-7,7-dimethyl-7-azoniabicyclo [2.2.1]heptane bromide

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / 1,4-dioxane / 0.5 h / 20 °C

1.2: pH 10

2.1: water; sodium tris(acetoxy)borohydride / 1,2-dichloro-ethane / 20 °C

3.1: diethyl ether; acetone / 48 h / 20 °C

With hydrogenchloride; water; sodium tris(acetoxy)borohydride; In 1,4-dioxane; diethyl ether; 1,2-dichloro-ethane; acetone;