1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane

Base Information

Chemical Name:1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane
CAS No.:247076-34-2
Molecular Formula:C₄₄H₈₆B₂Li₂N₄O₄P₂Si
Molecular Weight:860.728
Hs Code.:

Synonyms:1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane

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Technology Process of 1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane

There total 1 articles about 1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109-72-8,29786-93-4
n-butyllithium

: 110-71-4
1,2-dimethoxyethane

: 235756-34-0
(((CH₃)2CH)2N)2BP(H)Li(CH₃OCH₂CH₂OCH₃)

: 80-10-4
diphenylsilyl dichloride

: 247076-34-2
1,2-bis(lithiodimethoxyethane)-([bis(diisopropylamino)boryl]phosphino)diphenylsilane

Guidance literature:: In 1,2-dimethoxyethane; hexane; byproducts: LiCl; inert atmosphere; mixing stoich. amts. of Si- and B-compds. in hexane at0°C, stirring at 23°C for 5 h, evapn., dissoln. in DME, a ddn. of BuLi (in hexane) at -78°C, stirring (-78°C, 2 h; then 23°C, 16 h); filtration, evapn. (reduced pressure), washing (cold hexane); elem. anal.;