tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate

Base Information

• Chemical Name: tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate
• CAS No.: 476416-78-1
• Molecular Formula: C₂₃H₃₀N₄O₅S₃
• Molecular Weight: 538.713

Synonyms:tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate

Chemical Property of tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate

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Technology Process of tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate

There total 1 articles about tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-[(1Z)-8-mercapto-5,6-dimethyl-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-1-ylidene]-4-methylbenzenesulfonamide (476414-52-5,607706-85-4) + 3-bromopropylamine tert-butylcarbamate (83948-53-2) → tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate (476416-78-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; Heating;

DOI:10.1016/j.chembiol.2009.12.012

Reference yield:

tert-butyl {3-[((1Z)-5,6-dimethyl-1-{[(4-methylphenyl)sulfonyl]imino}-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-8-yl)thio]propyl}carbamate (476416-78-1) → N-{(1Z)-8-[(3-aminopropyl)thio]-5,6-dimethyl-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-1-ylidene}-4-methylbenzenesulfonamide (476416-90-7)

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 1h;

DOI:10.1016/j.chembiol.2009.12.012

upstream raw materials:

N-[(1Z)-8-mercapto-5,6-dimethyl-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-1-ylidene]-4-methylbenzenesulfonamide

3-bromopropylamine tert-butylcarbamate

Downstream raw materials:

N-{(1Z)-8-[(3-aminopropyl)thio]-5,6-dimethyl-3-oxo-2,3-dihydro-1H-imidazo[5,1-c][1,4]thiazin-1-ylidene}-4-methylbenzenesulfonamide

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