4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

Base Information

Chemical Name:4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde
CAS No.:1354792-74-7
Molecular Formula:C₁₉H₁₅N₃O₄
Molecular Weight:349.346
Hs Code.:

Synonyms:4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

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Chemical Property of 4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

Chemical Property:

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Technology Process of 4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

There total 3 articles about 4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1254035-93-2
1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)-azetidin-3-yl methanesulfonate

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1354792-74-7
4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

Guidance literature:: With caesium carbonate; In N,N-dimethyl acetamide; at 110 ℃; for 5h; Product distribution / selectivity;

Reference yield:

: 16691-25-1
ethyl 5-phenyl-1,3,4-oxadiazole-2-carboxylate

: 1354792-74-7
4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; sodium cyanide / methanol / 0.33 h / 20 °C

2: triethylamine / dichloromethane / Cooling with ice

3: caesium carbonate / N,N-dimethyl acetamide / 5 h / 110 °C

With sodium cyanide; caesium carbonate; triethylamine; In methanol; dichloromethane; N,N-dimethyl acetamide;

Reference yield:

: 1254035-92-1
(3-hydroxyazetidin-1-yl)(5-phenyl-1,3,4-oxadiazol-2-yl)methanone

: 1354792-74-7
4-(1-(5-phenyl-1,3,4-oxadiazole-2-carbonyl)azetidin-3-yloxy)benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / Cooling with ice

2: caesium carbonate / N,N-dimethyl acetamide / 5 h / 110 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl acetamide;