Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

Base Information

Chemical Name:Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester
CAS No.:1026598-44-6
Molecular Formula:C₃₃H₄₀N₂O₈
Molecular Weight:592.689
Hs Code.:

Synonyms:Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

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Chemical Property of Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

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Technology Process of Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

There total 6 articles about Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 144690-06-2
4-acetyl-2-propylimidazole-5-carbonitrile

: 1026598-44-6
Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 6N aq. HCl / 8 h / Heating

2: HCl / 16 h / Ambient temperature

3: 87 percent / NaBH₄ / ethanol / 0.5 h

4: 1.) t-BuOK / 1.) DMA, 0 deg C, 10 min, 2.) DMA, RT, 1 h

5: Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm950450f

Reference yield:

: 1025972-83-1
4-acetyl-2-propylimidazole-5-carboxylic acid

: 1026598-44-6
Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: HCl / 16 h / Ambient temperature

2: 87 percent / NaBH₄ / ethanol / 0.5 h

3: 1.) t-BuOK / 1.) DMA, 0 deg C, 10 min, 2.) DMA, RT, 1 h

4: Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; potassium tert-butylate; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm950450f

Reference yield:

: 144690-08-4
ethyl 4-(1-hydroxyethyl)-2-propylimidazole-5-carboxylate

: 1026598-44-6
Oxalic acid 1-[1-(2'-tert-butoxycarbonyl-biphenyl-4-ylmethyl)-5-ethoxycarbonyl-2-propyl-1H-imidazol-4-yl]-ethyl ester ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) t-BuOK / 1.) DMA, 0 deg C, 10 min, 2.) DMA, RT, 1 h

2: Et₃N / CH₂Cl₂ / 0.5 h / Ambient temperature

With potassium tert-butylate; triethylamine; In dichloromethane;
DOI:10.1021/jm950450f