dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

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Chemical Name:dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester
CAS No.:946125-72-0
Molecular Formula:C₁₉H₁₉N₃O₄
Molecular Weight:353.378
Hs Code.:

Synonyms:dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

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Technology Process of dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

There total 4 articles about dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 946132-31-6
dimethyl-carbamic acid 4-methyl-3-(3-nitrobenzyl)-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

: 946125-72-0
dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

Guidance literature:: With tin(II) chloride hydrate; In ethyl acetate; at 20 ℃; for 4h; Reflux;
DOI:10.1021/ml400379x

Reference yield:

: 946125-89-9
7-hydroxy-4-methyl-3-(3-nitrobenzyl)-pyrano[2,3-b]pyridin-2-one

: 946125-72-0
dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

1.2: 2 h / 100 °C

2.1: tin(II) chloride hydrate / ethyl acetate / 4 h / 20 °C / Reflux

With tin(II) chloride hydrate; sodium hydride; In ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ml400379x

Reference yield:

: 626-06-2
2,6-dihydroxypyridine

: 946125-72-0
dimethylcarbamic acid 3-(3-aminobenzyl)-4-methyl-2-oxo-2H-pyrano[2,3-b]pyridin-7-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: zinc trifluoromethanesulfonate / methanol / 30 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

2.2: 2 h / 100 °C

3.1: tin(II) chloride hydrate / ethyl acetate / 4 h / 20 °C / Reflux

With tin(II) chloride hydrate; zinc trifluoromethanesulfonate; sodium hydride; In methanol; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ml400379x