2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Base Information

Chemical Name:2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide
CAS No.:123420-23-5
Molecular Formula:C₄₁H₄₅NO₃P*I
Molecular Weight:757.691
Hs Code.:

Synonyms:2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

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Technology Process of 2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

There total 1 articles about 2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 101-06-4
N,N-dibenzyl-2-aminoethanol

: 82777-75-1
1-<(2-Methyl-1,3-dioxolan-2-yl)methyl>ethenyltriphenylphosphonium iodide

: 123420-23-5
2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Guidance literature:: n-butyllithium; In diethyl ether; for 120h; Ambient temperature;
DOI:10.1055/s-1989-27232

Reference yield: 95.0%

: 123420-23-5
2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

: 123420-24-6
2-(2-Benzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In methanol; for 9h; Ambient temperature;
DOI:10.1055/s-1989-27232

Reference yield:

: 123420-23-5
2-(2-Dibenzylaminoethoxy)-1-<(2-methyl-1,3-dioxolan-2-yl)methyl>ethyltriphenylphosphonium iodide

: 123420-27-9
3-Acetonyl-4-benzylmorpholine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂, conc. aq. HCl / 10percent Pd/C / methanol / 9 h / Ambient temperature

2: 4 N aq. H₂SO₄ / acetone / 48 h / Heating

3: Et₃N / H₂O; acetone / 24 h / Ambient temperature

With hydrogenchloride; sulfuric acid; hydrogen; triethylamine; palladium on activated charcoal; In methanol; water; acetone;
DOI:10.1055/s-1989-27232