1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

Base Information

Chemical Name:1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole
CAS No.:438623-98-4
Molecular Formula:C₂₂H₂₅NO₂
Molecular Weight:335.446
Hs Code.:

Synonyms:1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

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Technology Process of 1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

There total 7 articles about 1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 438623-97-3
2-acetyl-1-benzyl-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

: 438623-98-4
1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 2h;
DOI:10.1021/jm0401309

Reference yield:

: 77-92-9,906507-37-7
citric acid

: 438623-97-3
2-acetyl-1-benzyl-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

: 438623-98-4
1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

Guidance literature:: With sodium borohydrid; In ethanol; ethyl acetate;

Reference yield:

: 1730-48-9
6-methoxy-1,2,3,4-tetrahydronaphthalene

: 438623-98-4
1-benzyl-2-(1-hydroxyethyl)-4-methoxy-6,7,8,9-tetrahydro-1H-benz[g]indole

Guidance literature:: Multi-step reaction with 6 steps

1.1: POCl₃ / 0.5 h / 0 °C

1.2: 53 percent / 4 h / 80 °C

2.1: 52 percent / NaOEt / diethyl ether; ethanol / 2 h / -10 °C

3.1: 83 percent / rhodium(II) acetate dimer / toluene / 5 h / Heating

4.1: NaH / dimethylformamide

4.2: 37 percent / dimethylformamide / 45 h

5.1: tetrahydrofuran; toluene / 1 h / 2 °C

5.2: aq. NaOH / tetrahydrofuran; toluene; diethyl ether / 0.5 h

5.3: 73 percent / aq. HCl / acetone; CH₂Cl₂ / 0.33 h

6.1: 100 percent / NaBH₄ / ethanol / 2 h

With dirhodium tetraacetate; sodium tetrahydroborate; sodium ethanolate; sodium hydride; trichlorophosphate; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide; toluene; 1.2: Vilsmeier reaction;
DOI:10.1021/jm0401309