ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

Base Information

Chemical Name:ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate
CAS No.:1349807-48-2
Molecular Formula:C₂₀H₂₃N₃O₅S
Molecular Weight:417.486
Hs Code.:

Synonyms:ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

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Chemical Property of ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

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Technology Process of ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

There total 5 articles about ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.62%

: 1349808-14-5
1-(4-amino-3-methylphenylsulfonyl)-5-methyl-4-phenylimidazolidin-2-one

: 541-41-3
chloroformic acid ethyl ester

: 1349807-48-2
ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

Guidance literature:: With pyridine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmcl.2011.09.025

Reference yield:

: 1349808-06-5
2,2,2-trifluoro-N-(4-(2-methoxy-5-methyl-4-phenyl-4,5-dihydroimidazol-1-ylsulfonyl)-2-methylphenyl)acetamide

: 1349807-48-2
ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol / 0 °C

2: hydrogenchloride / diethyl ether / 3 h / 20 °C

3: pyridine / dichloromethane / 20 °C

With pyridine; hydrogenchloride; sodium hydroxide; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2011.09.025

Reference yield:

: 1349808-34-9
C₁₁H₁₄N₂O

: 1349807-48-2
ethyl 2-methyl-4-((4S)-5-methyl-2-oxo-4-phenylimidazolidin-1-ylsulfonyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / water; acetone

2: sodium hydroxide / ethanol / 0 °C

3: hydrogenchloride / diethyl ether / 3 h / 20 °C

4: pyridine / dichloromethane / 20 °C

With pyridine; hydrogenchloride; sodium hydrogencarbonate; sodium hydroxide; In diethyl ether; ethanol; dichloromethane; water; acetone;
DOI:10.1016/j.bmcl.2011.09.025