1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

Base Information

Chemical Name:1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate
CAS No.:1579250-18-2
Molecular Formula:C₁₉H₂₃N₂*F₆P
Molecular Weight:424.369
Hs Code.:

Synonyms:1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

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Chemical Property of 1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

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Technology Process of 1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

There total 3 articles about 1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 72991-60-7
N¹,N²-bis(2,6-dimethylphenyl)ethane-1,2-diamine

: 149-73-5
trimethyl orthoformate

: 1579250-18-2
1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

Guidance literature:: N¹,N²-bis(2,6-dimethylphenyl)ethane-1,2-diamine; With hydrogenchloride; In diethyl ether; at 20 ℃; for 0.25h;

trimethyl orthoformate; In toluene; at 90 ℃; for 16h;

With potassium hexafluorophosphate; In methanol; water; at 20 ℃; for 2h;
DOI:10.1021/jo500068p

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 1579250-18-2
1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 12 h / 0 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 48 h / 0 - 70 °C

3.1: hydrogenchloride / diethyl ether / 0.25 h / 20 °C

3.2: 16 h / 90 °C

3.3: 2 h / 20 °C

With pyridine; hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo500068p

Reference yield:

: 91325-47-2
N,N’-bis(2,6-dimethylphenyl)oxalamide

: 1579250-18-2
1,3-bis(2,6-dimethylphenyl)imidazolinium hexafluorophosphate

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 48 h / 0 - 70 °C

2.1: hydrogenchloride / diethyl ether / 0.25 h / 20 °C

2.2: 16 h / 90 °C

2.3: 2 h / 20 °C

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo500068p